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BS 6043-2-18:2001

$102.76

Methods of sampling and test for carbonaceous materials used in aluminium manufacture – Electrode coke – Determination of total sulfur by the Eschka method

Published By Publication Date Number of Pages
BSI 2001 16
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This International Standard specifies a reference method for determining the total sulfur content of calcined coke and calcined carbon products by the Eschka method, provided that they contain a minimum of 0.1 % by mass and preferably less than 4 % by mass of sulfur.

PDF Catalog

PDF Pages PDF Title
3 Carbonaceous materials used in the production of aluminium�— Calcined coke and calcined carbon pr…
5 Contents Page
6 Foreword
7 Introduction
9 Carbonaceous materials used in the production of aluminium�— Calcined coke and calcined carbon pr…
1��� Scope
2��� Normative references
3��� Principle
4��� Reagents
4.1��� Eschka mixture
4.2��� Hydrochloric acid
10 4.3��� Potassium sulfate
4.4��� Barium chloride
4.5��� Methyl red
4.6��� Ammonia
4.7��� Silver nitrate
5��� Apparatus
5.1��� Analytical balance
5.2��� Graduated glassware
5.3��� Electrically heated muffle furnace
5.4��� Crucible
5.5��� Flat plate
5.6��� Gooch crucible
5.7��� Air oven
5.8��� Filter paper
5.9��� Dessicator
11 6��� Preparation of test sample
7��� Procedure
7.1��� Test portion
7.2��� Loading the crucible
7.3��� Ignition
7.4��� Recovering the residue
7.5��� Extraction
12 7.6��� Precipitation of barium sulfate
7.7��� Blank
8��� Expression of results
13 9��� Precision
9.1��� General
9.2��� Repeatability,
9.3��� Reproducibillty,
10��� Test report
14 Derivation of factors used in the calculation in clause�
15 Bibliography
BS 6043-2-18:2001
$102.76