BS 6043-2-18:2001
$102.76
Methods of sampling and test for carbonaceous materials used in aluminium manufacture – Electrode coke – Determination of total sulfur by the Eschka method
Published By | Publication Date | Number of Pages |
BSI | 2001 | 16 |
This International Standard specifies a reference method for determining the total sulfur content of calcined coke and calcined carbon products by the Eschka method, provided that they contain a minimum of 0.1 % by mass and preferably less than 4 % by mass of sulfur.
PDF Catalog
PDF Pages | PDF Title |
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3 | Carbonaceous materials used in the production of aluminium�— Calcined coke and calcined carbon pr… |
5 | Contents Page |
6 | Foreword |
7 | Introduction |
9 | Carbonaceous materials used in the production of aluminium�— Calcined coke and calcined carbon pr… 1��� Scope 2��� Normative references 3��� Principle 4��� Reagents 4.1��� Eschka mixture 4.2��� Hydrochloric acid |
10 | 4.3��� Potassium sulfate 4.4��� Barium chloride 4.5��� Methyl red 4.6��� Ammonia 4.7��� Silver nitrate 5��� Apparatus 5.1��� Analytical balance 5.2��� Graduated glassware 5.3��� Electrically heated muffle furnace 5.4��� Crucible 5.5��� Flat plate 5.6��� Gooch crucible 5.7��� Air oven 5.8��� Filter paper 5.9��� Dessicator |
11 | 6��� Preparation of test sample 7��� Procedure 7.1��� Test portion 7.2��� Loading the crucible 7.3��� Ignition 7.4��� Recovering the residue 7.5��� Extraction |
12 | 7.6��� Precipitation of barium sulfate 7.7��� Blank 8��� Expression of results |
13 | 9��� Precision 9.1��� General 9.2��� Repeatability, 9.3��� Reproducibillty, 10��� Test report |
14 | Derivation of factors used in the calculation in clause� |
15 | Bibliography |